0123 The shear bond strength of three luting agents to ceramic
S. REICH, M. WICHMANN, and M. TROELTZSCH, University of Erlangen-Nuremberg, Germany

Objectives: The aim of this study was to evaluate the shear bond strength of three luting agents to a machinable feldspatic ceramic under different pretreatment methods of the ceramic material.

Methods: RelyX Unicem (3M ESPE), Calibra (Dentsply) and Variolink (Ivoclar-Vivadent) were used as resin cements. They were bonded to machine milled feldspatic ceramic disks, which were pretreated in five different ways: [A]: no pretreatment of the ceramic; [B]: ceramic etched with HF; [C]: silanizing; [D]: ceramic etched and silanized; [E]:ceramic etched with HF, silanized and treated with Heliobond (Ivoclar-Vivadent). The shear bond strength of 10 specimens per material and per ceramic pretreatment were tested initially, after 5*103 thermocycles and after 104 thermocycles. Results: Mean values of shear bond strength in MPa:

ceramic treatment

[A]

[B]

[C]

tested at:

initial

5*103

104

initial

5*103

104

initial

5*103

104

Calibra

4,41

**

**

7,41

11,2

9,81

3,31,2

**

**

Variolink

5,4

6,1

**

9,6

9,4

9,42

12,51

16,8

18,4

Unicem

6,71

5,9

8,3

9,91

13,8

15,11,2

12,22

15,6

12,4

ceramic treatment

[D]

[E]

tested at:

initial

5*103

104

initial

5*103

104

Calibra

7,401,2

10,71,2

10,31,2

12,0

15,51

11,11,2

Variolink

17,61,3

15,11,3

18,61

16,8

24,81

25,01

Unicem

12,82,3

22,22,3

20,92

12,5

20,4

24,32

** = debonding during thermocycling

The superscript letters within the same column indicate a significant difference according to the U-test at p £ .05, (Bonferroni corrected).

Conclusion: Due to the results of this study a simplification of ceramic treatment in combination with Variolink and RelyX Unicem seems to be possible. For the Calibra material only the complete pretreatment procedure [E] should be used and lead to reliable adhesion values.

Seq #16 - Dental Materials: Ceramics and Luting Materials
9:00 AM-11:00 AM, Friday, 27 August 2004 Crowne Plaza Hotel SEDIR II

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