0890 Dynamic Fatigue of Dental Ceramics
C.C. GONZAGA1, P.F. CESAR1, W.G. MIRANDA1, and H.N. YOSHIMURA2, 1University of Sao Paulo, Brazil, 2Institute of Technological Research of the State of São Paulo, Brazil

Objective: To compare the stress corrosion susceptibility coefficient (ns) of two dental porcelains (D and V) and two glass-ceramics (E1 and E2) using dynamic fatigue test. Methods: 60 discs (1mm-thick and diameter of 12mm) of each material were constructed according to manufacturers' processing methods. After that they were ground and polished to their final dimensions. The ns values were obtained by dynamic fatigue test, using a biaxial flexural strength fixture (piston-on-three-balls) and five constant stress rates (0.01, 0.1, 1, 10, and 100 MPa/s, n=10). During the tests, specimens were immersed in artificial saliva at 37oC. Inert strength (IS) was determined at 100 MPa/s in silicon oil (n=10). Linear regression analysis of log stress rate versus log strength was performed to calculate ns, considering that the slope of the curve was 1/(ns+1). Results: E2 showed the lowest ns. E1 and V showed similar ns values, which were higher than that of porcelain D. As to flexural strength, the highest values were obtained for E2, followed by E1, V and D regardless of the stress rate. The mean strength of the materials obtained at 100 MPa/s in artificial saliva was 64 to 80% lower than the IS. Conclusion: E2 is more susceptible to slow crack propagation than the other materials tested. E1 and V responded similarly with respect to slow crack growth; however they were less susceptible to this phenomenon than porcelain D. Acknowledgments: FAPESP, CNPq and CAPES.

Material

Mean fracture strength (MPa)

IS (MPa)

ns

0.01MPa/s

0.1MPa/s

1MPa/s

10MPa/s

100MPa/s

D

(d.Sign/Ivoclar)

40.8±3.3

42.1±2.8

46.8±4.9

58.4±4.2

60.1±6.8

94.2±9.4

20.4

V

(VM7/Vita)

62.5±11.3

65.6±11.9

70.8±15.2

78.8±11.3

88.5±19.7

123.4±21.6

26.8

E1

(Empress/Ivoclar)

86.3±11.2

95.5±8.2

98.9±12.2

115.0±15.7

118.1±16.1

166.9±21.7

29.7

E2

(Empress-2/Ivoclar)

151.1±12.6

160.3±13.9

180.6±19.7

216.4±22.8

246.4±29.8

307.3±38.4

17.1

Seq #107 - Ceramics: Mechanical Properties and Marginal Fit
3:30 PM-4:45 PM, Thursday, March 22, 2007 Ernest N. Morial Convention Center Exhibit Hall I2-J
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