0328 Bonding to alumina reinforced ceramic: adhesion methods and their durability
F.P.P. LEITE, T.S. GOIA, L.F. VALANDRO, G. SAAVEDRA, V.Z.C. VÁSQUEZ, O. MUTLU, M.A. BOTTINO, and E.T. KIMPARA, Universidade Est. Paulista Julio Mesquita, São José dos Campos, Brazil

Objectives:In this study was evaluated the bond durability of a composite resin for repair to an alumina reinforced ceramic , submitted to 2 different surfaces treatments. Methods:There were made 32 ceramic blocks (Vitadur-á)(5x5x5mm), as recommended by manufacturer, that were randomly separated into 2 groups, considering the surface treatment (ST): (ST-1) Silica sandblasting with 30ìm particles (CoJet – Sand) + silane (ESPE-Sil); (TS-2) Conditioning with fluoric acid 10%1m + silane (ESPE-Sil). Further on mono-component adhesive (Single Bond, 3M-Espe) on the ceramic surface and 3 layers of a composite resin measuring ± 1,5 mm (W3D Master, Wilcos) were applied. The samples were sectioned in the x and y axis, resulting in 10 specimens (sp) per ceramics block (adhesive area of ± 1mm²). The sp of each block were divided into 2 subgroups, according to the storage. Four experimentals groups (n=8) were obtained: G1) ST-1 + immediate essay [IE]; G2) ST-1 + thermocycling (6000 cycles, 5°-55°C) [TC]; G3) ST-2 + IE; G4) ST-2 + TC. Each sp were fixed with cyanoacrylate on adapted caliper, and the tensile test was performed (1mm/min). Results: The obtained data (Mpa) were evaluated by 2 way ANOVA and Tukey (á=0.05). G1 (12,30±2,93a), G2 (14,47±2,22a) and G4 (12,08±1,89a) presented bond durability statistically similar among G1, G2 and G4, which were lowest than G3 (19,80±2,28b) (p<0,001). The surface treatments were similar among G1,G2 and G4 (p=0,061). The thermocycling reduced the bond durability in ST-2 (p=0,041). Conclusion: The silica coating and acid conditioning showed similar bond strength.

Seq #58 - Adhesives, Bonding, Surface Treatments, Physical Properties
2:00 PM-3:00 PM, Thursday, 9 March 2006 Dolphin Hotel Pacific Hall
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