3130 Bonding of Paint Resin onto Prosthetic Resin Composite
K. MURAGUCHI1, S. SUZUKI2, H. MINAMI1, and T. TANAKA1, 1Kagoshima University, Japan, 2University of Alabama, Birmingham, USA

Introduction: A resin-paint has been developed to modify the shade of completed resin composite prostheses at chair side. This study evaluated the bond strength of the resin-paint to a prosthetic resin composite after cyclic thermal stressing. Materials and methods: The resin-paint (Master Palette, Kulzer) used was a flowable resin containing 40wt% fillers. A resin composite (Dentacolor Sirius, Kulzer) was photo-polymerized into a disc shape (10mm diameter, 3mm high). Bonding surfaces of the disc specimens were polished with a 600-grit Si-C paper and pre-treated with; 1) immersion in methylene chloride (MC), 2) airborne particle abrasion with 50µm aluminum oxide (AB), 3) application of CB liquid (Kulzer) after AB (CB), and 4) application of EG-bond (Sun Medical) after AB (EG). A piece of tape with 5 mm diameter opening was used to provide bonding area. The resin-paint was applied (0.5 mm thick) and photo-polymerized, then Dentacolor Sirius was photo-polymerized (6mm diameter, 2.0mm thickness) onto it as a loading handle. Shear bond strengths were measured at a 1.0 mm/min crosshead speed before and after thermo-cycling (4-60, 50,000cycles). All data were statistically analyzed by 2-way ANOVA and Scheffe’s F-test (p<0.05). Results: The shear bond strengths for each group are presented in the table. Bond strengths of groups CB and EG were significantly higher than that of group AB after 50,000 thermo-cycles (p<0.05). Conclusions: Applications of CB liquid and EG-bond after airborne particle abrasion are effective to obtain better bonding of the resin-paint.

Table. Shear bond strengths of each group; Mean (SD), Unit: MPa, n=5.

MC

AB

CB

EG

Before thermo-cycling

6.0 (2.2)

17.9 (2.2) a, b

22.9 (2.2) a, c

20.3 (2.1) a, d

After 50,000 thermo-cycles

0

14.5 (1.9) b

18.6 (2.2) c, e

16.6 (0.5) d, e

Values with the same alphabet were not significantly different (p>0.05).

Seq #335 - Adhesion III
10:15 AM-11:30 AM, Saturday, 13 March 2004 Hawaii Convention Center Exhibit Hall 1-2

Back to the Dental Materials: I - Adhesion-Composite Bond Strength Program
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