3129 Bond Strength of Adhesive Resin Cements to Tooth Structure
J.M. POWERS1, L.M. PINZON1, and M. KIMURA2, 1University of Texas Health Science Center at Houston Dental Branch, Houston Biomaterials Research Center, USA, 2Tokuyama Dental Corp, Tsukuba, Japan

Objective: To determine the tensile bond strengths of two adhesive resin cements in light- and self-cured modes to human enamel and superficial dentin at 10 m and 24 h.

Materials and Methods: Two adhesive resin cements [Bistite II DC, Tokuyama Dental (BDC); Panavia F, Kuraray America (PF)] were bonded as cones (3-mm bond diameter) to human enamel and dentin prepared with 600-grit surfaces. The cements were tested in light-cured (LC) and self-cured (SC) modes. Self-cured specimens were bonded using pre-cured composite cones (TPH Spectrum). Storage times before testing were 10 m and 24 h in water. Specimens were debonded in tension on Instron at crosshead speed of 0.5 mm/m. Results: Means (sd, n=8) of bond strength (MPa) and failure mode data are shown. Fisher's PLSD intervals (p<0.05) for cements, curing mode, substrates and time were each 2.0 MPa. Conclusions: Bond strengths of both cements increased with time. Self-cured polymerization resulted in higher bond strengths than the light-cured mode. Bond strength to enamel was higher than bond strength to dentin. BDC had equal or higher bond strengths to dentin than PF. Funded in part by Tokuyama Dental Corp.

Enamel/LC

Enamel/SC

10 min

24 hrs

10 min

24 hrs

BDC

13.9(4.5) 21A/79C*

20.1(6.7)  10A/90C

20.4(6.2) 15A/25CR/60I

23.2(7.9) 15A/73CR/12I

PF

13.9(3.7)    9A/91C

20.4(5.1)5A/83C/12T

20.2(7.5)28A/7CR/65I

26.7(7.9) 28A/44CR/12T/16I

Dentin/LC

Dentin/SC

10 min

24 hrs

10 min

24 hrs

BDC

10.7(4.1)  85A/15C

14.1(5.7)    94A/6C

14.3(5.5)    90A/10I

17.1(8.3)    89A/11I

PF

9.2(2.6)      95A/5C

11.8(3.1)    91A/9C

8.6(3.2)      89A/11I

11.2(4.8)78A/1C/21I

*A, adhesive failure between tooth and cement; C, cohesive failure in cement; CR, cohesive failure in composite; I, adhesive failure between composite and cement; T, cohesive failure in tooth

Seq #335 - Adhesion III
10:15 AM-11:30 AM, Saturday, 13 March 2004 Hawaii Convention Center Exhibit Hall 1-2

Back to the Dental Materials: I - Adhesion-Composite Bond Strength Program
Back to the IADR/AADR/CADR 82nd General Session (March 10-13, 2004)

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