1660 Influence of Powder-Liquid Mixing Ratio on Translucency and Apparent Density of a Dental Porcelain
A.W. BENHAM, J.A. GRIGGS, and Y. ZHANG, Baylor College of Dentistry (Texas A&M University System Health Science Center), Dallas, USA

Dental technicians employ a variety of techniques when condensing and layering dental porcelain. Differences in powder-liquid ratio may affect the physical properties of dental porcelain.  OBJECTIVE:  The purpose of this study was to determine if varying the powder-liquid ratio during condensation would affect the translucency and apparent density of incisal porcelain. METHODS: Eris incisal porcelain (shade A4) was mixed with deionized water in powder-liquid ratios of 2.56 g/mL, 2.78 g/mL, and 3.05 g/mL. The resulting slurry was condensed by vibration blotting to form four disk specimens (16 mm diameter x 2 mm thickness) per group that were fired under vacuum and polished to a final thickness of 1.10 ± 0.02 mm with a 3 mm finish.  The translucency of each specimen was taken as the contrast ratio of shade value (L*) on black and white backgrounds using a tristimulus colorimeter under immersion liquid with a refractive index of 1.5000. The apparent density of each specimen was calculated using Archimedes' method.  The specimens were electroplated with gold and observed under the SEM for visual comparison of pore size. RESULTS:  Mean data values (standard deviations) were:

Powder-Liquid Ratio (g/mL)

Apparent Density (g/cm3)

Contrast Ratio

2.56

 2.560 (0.006)

0.514 (0.007)

2.78

 2.579 (0.009)

0.579 (0.006)

3.05

 2.560 (0.005)

0.509 (0.004)

One-way ANOVA showed a significant effect of mixing ratio on apparent density (p = 0.005) but not on contrast ratio (p = 0.21). CONCLUSION: These data indicate that varying powder-liquid ratio had a significant effect only on apparent density of Eris incisal porcelain. This study was supported by the Baylor Oral Health Foundation and NIH-NIDCR grants DE13358 and DE01788.

Seq #207 - Ceramics: Surface Treatment, Surface Chemistry, and Bonding
11:00 AM-12:15 PM, Saturday, 15 March 2003 Henry B. Gonzalez Convention Center Exhibit Hall C

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