0448 Indentation Size Effect on the Hardness of Dental Ceramics
E. CHANG, and I. DENRY, The Ohio State University, Columbus, USA

Previous studies have shown that conventional hardness measurements are load-dependent. Hardness values obtained at low loads are usually very high, while at higher loads the hardness becomes constant. Objective: To determine the effect of indentation load on the Vickers hardness of three types of ceramic materials: a lithium disilicate-based ceramic (OPC 3G), a mica-based glass-ceramic (Dicor MGC) and a zirconia-based ceramic (Cercon zirconia). Soda lime glass was used as control. Method: Specimens of each material (n=5) were embedded in epoxy resin; polished; then indented at loads ranging between 1.96 and 98.1 N with a Vickers hardness tester (n=10 per load). For better accuracy indentation diagonals were measured directly from digital optical micrographs that were taken immediately after indentation. Hardness values were then calculated for each material. Results: ANOVA and Tukey's test showed that above a certain load, the hardness values were not significantly different for each material. The load corresponding to the transition point in the hardness vs. load curve was 4.9 N for both soda lime glass and the mica glass-ceramic, 19.6N for the lithium disilicate ceramic and 29.4N for the zirconia-based ceramic. Hardness values corresponding to the transition point were then compared between materials. The mean hardness of the zirconia-based ceramic (13.6 GPa at 29.4N) was significantly higher than that of the lithium disilicate-based ceramic (4.90 GPa at 19.6N), which was greater than that of the mica-based glass-ceramic (2.98 GPa at 4.9N) (p<0.05). The mean hardness obtained for soda lime glass compared favorably with previously published data (5.02 GPa at 4.9N). Conclusions: Statistically significant differences were observed for each material between the mean Vickers hardness at low loads and the mean Vickers hardness at high loads. The load needed to reach a constant hardness value varied with the material tested. Supported by NIH-NIDCR Grant No. DE 13570

Seq #65 - Ceramics: Strength and Fracture Analysis
1:45 PM-3:45 PM, Thursday, 13 March 2003 Henry B. Gonzalez Convention Center Room 206A

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