1282 Dimensional Change and Sorption of Dental Cements
W.W. JOHNSON1, D.A. COVEY1, M.P. WALKER2, W.W. BRACKETT3, and A. BUCKLEY1, 1 University of Nebraska College of Dentistry, Lincoln, USA, 2 University of Missouri, Kansas City School of Dentistry, USA, 3 University of Nebraska Medical Center College of Dentistry, Lincoln, USA

Objective: Previous studies have indicated hygroscopic expansion of luting agents occurs as a result of water sorption.  This expansion may initially compensate for setting contraction; however, further expansion has been linked to fracture of all-ceramic restorations.  The aim of this study was to determine time-dependent percent (%) volume change and %sorption of 6 luting agents.  Methods: Using mass measurements accurate to 0.001 gram, %sorption and %volume change were determined on luting agent specimens (n=6,10x2mm disks) stored at 37oC in distilled water.  The %volume change was determined using the hydrostatic principle, which assumes material buoyancy changes depend on volume change. Measurements were made at 1 day and 42 days.  The types of luting agents studied were resin cement (RC), resin-ionomer cement (RI), and glass ionomer cement (GIC). Results:

Material     

Time

%Sorption (SD)

%Expansion (SD)

Rely X ARC a,1

(RC)

1d

1.00  (0.22)

1.21  (1.66)

42d

1.78  (0.40)

1.63  (1.38)

Rely X Luting b,2,3

(RI)

1d

4.25  (0.75)

5.66  (3.69)

42d

4.60  (0.59)

6.31  (3.08)

Fuji I c,2

(GIC)

1d

5.50  (0.66)

5.79  (1.03)

42d

5.75  (0.54)

4.17  (0.99)

Fuji Cem b,3

(RI)

1d

4.24  (0.62)

7.44  (1.79)

42d

4.02  (0.93)

8.51  (0.78)

Fuji Plus c,4

              (RI)          

1d

6.14  (0.69)

11.08  (1.13)

42d

6.52  (0.52)

11.35  (1.29)

Advance c,4

(RI)

1d

5.50  (0.66)

14.65  (2.77)

42d

5.75  (0.54)

11.68  (2.54)

A 2-factor ANOVA (p£0.05)/Tukey's post hoc indicated that material was a significant factor for both %volume change and %sorption, while time was significant for %sorption only.  Post hoc subsets are indicated as a-c for % sorption and 1-4 for %expansion.  There was a positive correlation between %volume change and %sorption [Pearson's coefficient = 0.660 (p£0.01)].  Conclusion: All the luting agents showed an increase in sorption and volume; however, the resin cement showed the least increase.

Seq #163 - Other Ceramics and Cements
3:45 PM-5:00 PM, Friday, 14 March 2003 Henry B. Gonzalez Convention Center Exhibit Hall C

Back to the Dental Materials: III - Ceramics and Cements Program
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