| 3422 Effect of storage conditions on fracture toughness of a resin-modified glass ionomer cement | |||||||||||||||||||||||||||||||||||
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V.J. SETIEN, S.R. ARMSTRONG, and D.B. BOYER, The University of Iowa, Iowa City, USA The initial rapid photo-polymerization of resin-modified glass ionomers should make the on going acid base reaction less susceptible to any deleterious effects of water. Objective: This study evaluated the effect of maturation time and storage conditions on the fracture toughness of resin-modified glass ionomer (RMGI, Fuji II LC, GC America). Methods: Triangular molds (4x4x4x8 mm) were used to make 60 specimens, which were randomly divided into 5 groups. Light curing at 650 mW.cm-2 was performed 1 minute after mixing through a silicon-coated glass slide for 40 seconds, with an additional 40s light-cure from the bottom after removal from the mold. Fracture toughness (KQIvM) was determined according to the methods of Ruse et al. (J Biomed Mater Res 1996;31:457-463) with a crosshead speed of 0.3 mm/min. Group 1 was tested 4 minutes from the beginning of mixing, groups 2-5 were tested after being stored in 100%RH for either 1 or 3 days before transferring to artificial saliva or oil (Inland 45, Inland Vacuum Industries) for a total of 1 week storage at 37°C. Differences in fracture toughness were tested with ANOVA and Tukey (HSD) post-hoc at 95% confidence level. Results:
Conclusions: The photo-polymerization reaction may account for roughly half of the fracture toughness of RMGI based on immediate KQIvM data. Under the conditions of this study the exclusion of extrinsic water (oil) demonstrated no significant different effect on KQIvM.
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| Seq #312 - Cements, Bond Strength, Marginal Adaptation 11:00 AM-12:15 PM, Saturday, 9 March 2002 San Diego Convention Center Exhibit Hall C | |||||||||||||||||||||||||||||||||||
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Back to the Dental Materials: III - Ceramics and Cements Program
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